Development of enhanced methods for copper particles synthesis is crucial for the improvement of material science and technology. Therefore, in this study a successful synthesis of copper metal was achieved by chemical reduction. Ascorbic acid was used as a reducing agent. In the presence of soda, copper sulphate pentahydrated (CuSO4, 5H2O) with acid ascorbic at 60 °C of temperature produced metallic copper powder with the total degradation (100%) of copper ions (Cu2+). The presence of hydroxide ions (OH-) is necessary to achieve and improve the chemical reduction reaction. Several parameters, as reducing agent volume, reaction temperature and soda quantity were investigated and checked their impact in this research study. The obtained powder was washed and dried in the fresh air then analysed by X-ray diffraction